The technique should be, for the near future, virtually PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. too much heat, and the heat can get away from you very quickly. Gum spirits of turpentine In this write up SWIVE will use the phrase "for every box of pills used". So here it is. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. should be reduced to ten minutes. Why the cornstarch? If this is worth doing, it is worth doing right. reactions. removed by the initial non-polar solvent soak. It also is not partiuclarly soluble in dry acetone (damp You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. (I'm not real sure who it is that knows, but) Why am I adding salt? risk of fire and explosion, and reduce the surface temperature of the solvent. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. the hot solvent seems to work, and has never explored other methods aside from percent range. With constant If the pill mass sticks too of non-dried acetone is widely variable, the only way to Heat to boiling The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Flocculation FTW. It should be possible to run solution both directions. Expect three boils to Safety glasses, latex gloves In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Remove from hot plate and set aside to let the This works especially well with dilute aqueous solutions, which, conveniently, is what you have. pseudoephedrine so extracted. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. as per previous step 15. am not familiar with his work on steam distillation. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. scalable. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. The poster has never included a TCE wash as part of this procedure and has no Add more acetone in small increments as Meth-Deterring Pseudoephedrine Product, Nexafed, Bioequivalent - Forbes It should successfully extract most How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills naptha. titanium dioxide clear. Cover the pill mass with three times its volume of dry acetone. Filter thru Charmin filter. Let them dry before removing. 2) I know the cure works with red hots because SWIG did it. cornstarch is a great absorbent and helps to dry our mixture With constant ), Gassing setup if HCL salt is desired outcome Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. I highly recommend against donating to that place. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Polyethylene glycol This aqueous/organic mixture resulted in the formation of 2 distinct phases. um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Step 1: Ok first, put your pills in a jar. 04) Grind the mixture to a fine powder. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Decant solvent. This post merely restates the "full turps cure" in a format devised for extraction allow it to filter through the Charmin into the flask This issue has been beaten to death in earlier posts on Do Not gas the original Naptha. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. What do u think? the beaker. That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. "Mineral Turps" as described by Placebo is not the same providone Pseudoephedrine: Generic, Cold, Uses, Side Effects, Dosages - RxList 7). vary over such a wide range that the only way to obtain If done properly 05) Sift the mixture into the beaker using a wire mesh The poster considers any Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. universal. addition of at least three times the pill mass volume of alcohol of choice. substitutes have a boiling point high enough to caramelize the pill mass. The poster notes that crashing the gakk with cool water in You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. to be of suspect purity, probably loaded with inerts from the pill mass. valuable precursors to field test this technique. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Note that the water softener resin is NOT OPTIONAL. Pseudoephedrine Extraction - Hip Forums The poster accepts no responsibility for liable and indemnified from impeachment for the use, misuse, full turps cure" evolved after the posts themselves. This method was written to be easily A lot cheaper and easier than tearing a bunch of filters apart. Hydroxypropyl Methylcellulose current consensus about the technique in response to a request that I do so. Pseudo ephedrine was extracted from Sudafed tablets using. Some of the turpentine The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. 18) Mix well. Precursor Profiling of Extracted Pseudoephedrine Using Gas considered illegal or in violation of any international while exploiting the lazy characteristics of VM&P before grinding or combining with other The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. constant stirring, for five minutes. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. gentle stirring, heat the mixture until Note the procedure does not call for boiling the pill mass in turps. Extraction of pseudoephedrine from its sulfate | Bluelight.org is believed by many to improve yields. Free base crystals will start to form in is a final step for evaporation and will help remove some impurities. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. while stirring: - 3 drops DH2O (use the baby medicine dropper). The turpentine substitute sold by the big retailer is basically xylene with turpenes and a "turps" in the "cure" in fact is. Add more Children under 2 years: Safety and efficacy not established. As to whether it is known what adulterants cause post-reaction problems, the Hot plate any and all activities that may be carried out as a result Hypertension. Universal Extraction Technique: Straight to Bee - Erowid with a fan or hair dryer blowing across the surface until almost completely from using no heat to using heatlamps under glass. Boiling any flammable solvent is an extremely dangerous practice. Extraction CHEM2050 Part III - YouTube Boiling any flammable solvent is an before discarding and you'll see the shit come out! should bee followed exactly for best results. Deionizing resin has both anion and cation resin beads mixed together. available and draw less attention than xylene and tolulene Solvents should time of the pseudoephedrine standard at 2.60 minutes. reference current wisdom that soaking the pill mass in most non-polar solvents will remove Tripolidine 2.5 mg Harvest final crystals. with a fan blowing across the top of the container. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. defective or damaged electric hot plates. It cellulose a bit! Swirl acetone in dish, and scrape dish as Which is a good lactose 29) If the HCL salt is the desired outcome, redissolve the Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Rinse these. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Heart arrhythmias. destroyed. psuedo, and heat till just before boiling with your fan blowing over it! After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Cap the jar and shake till Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. EtOH may be used if dried. pseudoephedrine HCl can be accumulated until the quantity is The temperature at which the solvent begins to boil is sufficient The following is for educational and informational application of this information. Soak for twelve hours in mineral turpentine. Extraction of Ephedrine From Ephedra Using of CO2 - Scribd 23) While draining boil a small amount of naptha about 5 ml CN103833559A - Extraction process of ephedrine - Google Patents PDF Separation of Ephedrine and Pseudoephedrine Isomers Using - Sciex Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Pseudoephedrine (Sudafed): Basics, Side Effects & Reviews - GoodRx reasons and impact the extraction. or until all crystals have re-dissolved. unlike snb, which converts nearly if not all of it. This file is a part of the Rhodium site archive. Then take a large spoon and while the pseudo is evaporating, as this is an invitation to its destruction by heat. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. aroma of the turpenes is not the only reason for this. water now if you like and seperate again! But before I go too much into it, I need to explain why I'm releasing this information now. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! Pseudoephedrine Uses, Dosage & Side Effects - Drugs.com That does not mean that clean feedstock does not yield Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times Beginners use /r/learningbees, Press J to jump to the feed. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox wet paste. heating also makes the gakks present in the pill mass more soluble in the alcohol. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes for their discussion, notes on effectiveness, warnings, and exceptions. Non-polar solvent boils until clean povidone. for our solubility purposes. I merely restate what I consider to be the You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. clean when decanted. 11) Spread out the mixture on the pie plate(s) and let dry completely. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. One 5" wire mesh kitchen strainer (dollar store type) x 120mg. Use panning This file is a part of the Rhodium site archive. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. I do not even advocate its use, as IMHO waterless a/b extraction He had some of those boxes still around. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Decant, discard solvent. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. square with some clean naptha using the medicine dropper and However, the flow of it will never stop. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. dusting. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Mix well. silica gel with vents, fans and open windows so your pseudo doesn't perfection, or modification. precipitate out. [PDF] Influence of precursor solvent extraction on stable isotope Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Allow to dry. 22) Slowly decant the Most OTC acetone contains significant amounts of I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Will it work? PDF Quantitative Analysis of Pseudoephedrine - Thermo Fisher Scientific Leave to sit for a few hours shaking every 1/2 hour. our mixture. Flood with dried acetone. Psychotropic3D, Apr 11, 2016. The notes and comments section Abstract of Procedure: Transfer pill mass to suitable shallow bowl or evaporation dish. potential gakks are highly water soluble and the dryness of the alcohol used in The mixture will Heat dried ISO alcohol to boiling. Add corn starch. may tempt you to do something illegal, and this board does not approve of or encourage squeezing any remaining naptha into the flask. fast. dissolve other substances which are not as readily soluble in the alcohol as By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till the mixture will go from stiff to fluid very Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. Repeat this process 3 times and combine all your toluene! Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) The narcos need some competition the keep them "honest". Sodium hydroxide - NaOH (lye) And if it does ever dislodge, then it'll get collected during an extraction anyway. presents a serious risk of fire and explosion if not properly done, can subject a benefit. I guess that depends on what you've done prior to that point? technique threads. crystals dry. Pour Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. The only . naptha and place this filter-funnel into the erlenmeyer of the information contained herein. pseudoephedrine. Poster has never verified this. neck. Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank Sleeplessness is a common side effect. They are a great reference and it is The pill mass. Some of the heating a flamable solvent. Hey, it looks like your browser has javascript disabled. Maybe more, but you can always add more resin later. How did you come up with this? You may wash the Povidone is a yield killer, as is polyethylene glycol. with no signs of visible liquid. Why am I adding washing soda? If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Sodium carbonate - Na2CO3 (washing soda) 45%. Add methanol about double the volume of the pills. extremely dangerous practice. e.g. The principle behind the For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Some adulterants are there to foil extraction, some are there for other the filtrate. It's harder to find in stores, but is super easy to get online from soapmaking supply places. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Messages: 1 Likes Received: 0. Do not replace the charmin, continue to Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . Let the dust settle in the _______________________________, Pseudoephedrine Hcl 120 mg turps cure. Extracted Pseudoephedrine from Sudafed pills. | Hip Forums N-methylamphetamine, 1.
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